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Design and Testing of Low Temperature Part of an UHV – SPM Microscope
Frolec, Jiří ; Vonka, J. ; Hanzelka, Pavel ; Králík, Tomáš ; Musilová, Věra ; Urban, Pavel
We have developed low temperature part of an ultra high vacuum scanning probe microscope (UHV-SPM) working at variable temperature within the range from 20 K to 700 K. To achieve the required temperature range, a flow cooling system using cryogenic helium (approximately 5 K) as a coolant was designed. The system consists of a flow cryostat and a flexible low-loss transfer line connecting a Dewar vessel with the flow cryostat. We have also tested liquid nitrogen (approximately 77 K) as an alternative low-cost coolant. Using nitrogen, the microscope can operate at temperatures of about 100 K and higher. As the flow of the coolant through the cryostat can cause thermally induced two-phase flow fluctuations resulting in instability in temperatures, preliminary tests were done in order to find ways of avoiding the temperature oscillations and optimising the cooling process.
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Factors Influencing Thermal Radiative Properties of Metals
Králík, Tomáš ; Hanzelka, Pavel ; Musilová, Věra ; Srnka, Aleš
Data on thermal absorptivity and emissivity are important for calculations of heat flows in cryogenic devices. Although thermal radiative properties of materials used in cryogenics are measured, published and used for more than sixty years we have noticed that sometimes users of that data don’t well understand the significance of individual factors influencing thermal radiative properties. The sensitivity of the thermal radiative properties of metals to the condition of the surface and the difficulty of measurement, especially at low temperatures is probably the reason of dispersion of the published values. The effect of the material and its purity, finishing (machining, mechanical or chemical polishing) and of the protective coatings or accidental layers (water, oxidation) on the thermal radiative properties is not always obvious. Influence of the material, surface treatment, roughness and layers on the surface is discussed on the basis of our 20 year experience with measurement of the emissivity and absorptivity in the range from 20 K to 300 K.
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Temperature Inversion and Heat Transport Against the Temperature Drop in Two-Phase Convection of Cryogenic Helium
Urban, Pavel ; Schmoranzer, D. ; Hanzelka, Pavel ; Skrbek, L.
In the system of two bodies A and B connected by a two-phase vapour-liquid system consisting only of cryogenic helium, we observed anomalous heat transport from the colder but heated body B to the warmer but cooled body A. We noticed this effect during the process of liquid evaporation inside a cylindrical pressure convection cell used for study of Rayleigh-Bénard convection. This anomalous heat transfer occurs under non-equilibrium conditions, owing to the phase transitions that take place inside the cell while temperature inversion develops between the heated but cooler bottom plate and the cooled but warmer top plate. This process is, by virtue of the system being open with respect to heat transport, in no contradiction to the second law of thermodynamics, and a numerical model was formulated that describes the observations with good agreement.
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